Analysis of anthraquinones in Rumex crispus by micellar electrokinetic chromatography

Başkan S., DAUT-OZDEMIR A., GÜNAYDIN K., Erim F. B.

TALANTA, cilt.71, sa.2, ss.747-750, 2007 (SCI-Expanded) identifier identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 71 Sayı: 2
  • Basım Tarihi: 2007
  • Doi Numarası: 10.1016/j.talanta.2006.05.018
  • Dergi Adı: TALANTA
  • Derginin Tarandığı İndeksler: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Sayfa Sayıları: ss.747-750
  • Anahtar Kelimeler: Rumex crispus, anthraquinones, capillary electrophoresis, MEKC, CAPILLARY-ZONE-ELECTROPHORESIS, RHUBARB ANTHRAQUINONES, ACTIVE COMPONENTS, SODIUM CHOLATE, SEPARATION, CYCLODEXTRIN, DERIVATIVES, BIANTHRONES, LIQUID, AGENTS
  • İstanbul Teknik Üniversitesi Adresli: Evet

Özet

A micellar electrochromatographic method was performed for the analysis of the pharmaceutically important anthraquinones from the root of Rumex crispus. The separation of 1,5-dihydroxy-3-methylanthraquinone (1); 1, 3,5-trihydroxy-6-hydroxymethylanthraquinone (2); 1,5-dihydroxy-3-methoxy-7-methylanthraquinone (3) was achieved in 6 min using a running buffer containing 10 mmol/l sodium borate, 50 mmol/l sodium dodecylsulfate, and 25% acetonitrile at pH 10.6. The method is simple, rapid, and reproducible. (c) 2006 Elsevier B.V. All rights reserved.