Atıf İçin Kopyala
Başkan S., DAUT-OZDEMIR A., GÜNAYDIN K., Erim F. B.
TALANTA, cilt.71, sa.2, ss.747-750, 2007 (SCI-Expanded)
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Yayın Türü:
Makale / Tam Makale
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Cilt numarası:
71
Sayı:
2
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Basım Tarihi:
2007
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Doi Numarası:
10.1016/j.talanta.2006.05.018
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Dergi Adı:
TALANTA
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Derginin Tarandığı İndeksler:
Science Citation Index Expanded (SCI-EXPANDED), Scopus
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Sayfa Sayıları:
ss.747-750
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Anahtar Kelimeler:
Rumex crispus, anthraquinones, capillary electrophoresis, MEKC, CAPILLARY-ZONE-ELECTROPHORESIS, RHUBARB ANTHRAQUINONES, ACTIVE COMPONENTS, SODIUM CHOLATE, SEPARATION, CYCLODEXTRIN, DERIVATIVES, BIANTHRONES, LIQUID, AGENTS
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İstanbul Teknik Üniversitesi Adresli:
Evet
Özet
A micellar electrochromatographic method was performed for the analysis of the pharmaceutically important anthraquinones from the root of Rumex crispus. The separation of 1,5-dihydroxy-3-methylanthraquinone (1); 1, 3,5-trihydroxy-6-hydroxymethylanthraquinone (2); 1,5-dihydroxy-3-methoxy-7-methylanthraquinone (3) was achieved in 6 min using a running buffer containing 10 mmol/l sodium borate, 50 mmol/l sodium dodecylsulfate, and 25% acetonitrile at pH 10.6. The method is simple, rapid, and reproducible. (c) 2006 Elsevier B.V. All rights reserved.