Atomic absorption spectrometric determination of copper, cobalt, cadmium, lead, nickel and chromium in table salt samples after preconcentration on activated carbon


SOYLAK M., NARİN İ., Elci L., Dogan M.

KUWAIT JOURNAL OF SCIENCE & ENGINEERING, cilt.28, sa.2, ss.361-370, 2001 (SCI İndekslerine Giren Dergi) identifier identifier

  • Yayın Türü: Makale / Tam Makale
  • Cilt numarası: 28 Konu: 2
  • Basım Tarihi: 2001
  • Dergi Adı: KUWAIT JOURNAL OF SCIENCE & ENGINEERING
  • Sayfa Sayıları: ss.361-370

Özet

Copper, cobalt, cadmium, lead, nickel, and chromium contents of table salt samples were determined by atomic absorption spectrometry after preconcentration/separation on an activated carbon column as pyrocatechol violet (PV) complexes. The PV-metal ion complexes buffered to pH 6 were retained on an activated carbon column and were then eluted from the column with 1 M nitric acid in acetone. The effect of matrix ions on recoveries of the working elements was also examined. The recoveries of metal ions were in the range of 95-103%. The relative standard deviations (RSD) of the metal ion determinations varied from 2 to 9%.