Phosphorous esters of 2,13-dihydroxy-7a,14c-dihydronaphtho[1 ',2 ': 4,5]furo[3,2-d]furan

Kizilcan N., AKAR A., Talinli N., YASLAK S.

HETEROCYCLIC COMMUNICATIONS, vol.5, no.1, pp.27-30, 1999 (SCI-Expanded) identifier identifier

  • Publication Type: Article / Article
  • Volume: 5 Issue: 1
  • Publication Date: 1999
  • Doi Number: 10.1515/hc.1999.5.1.27
  • Journal Name: HETEROCYCLIC COMMUNICATIONS
  • Journal Indexes: Science Citation Index Expanded (SCI-EXPANDED), Scopus
  • Page Numbers: pp.27-30
  • Istanbul Technical University Affiliated: Yes

Abstract

2,13-dihydroxy-7a,14c-dihydronaphtho[1',2':4,5]furo[3.2-d]furan prepared from glyoxal bisulphite and 2,7-dihydroxynaphthalene was reacted with, C6H5PCl2, C6H5POCl2 and Br-C6H4OPOCl2 to produce its phosphorous esters. The structures of the products were investigated by MS, FTIR, H-1-NMR, C-13-NMR, and P-31-NMR. Although C6H5PCl2 gave a compound with a new ring containing phosphorous atom, C6H5POCl2 and Br-C6H4OPOCl2 resulted acyclic phosphorous esters.